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Unit I · Textile fibres
9 min readConcept sheetOften a 10-mark answer; the burning test comes as a 5-mark question

Classification and identification of textile fibres

Fibres are natural or man-made. Natural fibres are cellulosic, protein or mineral; man-made are regenerated or synthetic. A burning test sorts an unknown fibre into its group.

Textile fibreA fine, hair-like unit, far longer than it is wide, that can be spun into yarn
Only natural filamentSilk
Natural groupsCellulosic (plant), protein (animal), mineral
Man-made groupsRegenerated (from natural polymers) and synthetic (from petrochemicals)

Classification of textile fibres

GroupSub-groupExamples
Natural: cellulosic (plant)Seed hairsCotton, kapok
Natural: cellulosic (plant)Bast (stem) fibresFlax (linen), jute, hemp, ramie
Natural: cellulosic (plant)Leaf and fruit fibresSisal and pineapple (leaf); coir from coconut husk (fruit)
Natural: protein (animal)Wool and hairSheep's wool; specialty hair such as pashmina (cashmere), mohair, camel hair, angora rabbit
Natural: protein (animal)SecretionSilk: mulberry, tasar (tussar), eri and muga
Natural: mineralRock fibreAsbestos (no longer used, because its dust causes lung disease)
Man-made: regeneratedCelluloseViscose rayon, cuprammonium rayon, modal, lyocell; acetate and triacetate (modified cellulose)
Man-made: regeneratedProteinCasein (milk) and soya or corn protein fibres (azlon)
Man-made: syntheticBuilt from petrochemicalsNylon (polyamide), polyester, acrylic, polypropylene (olefin), spandex (elastane)
Man-made: inorganicMineral or metalGlass fibre, metallic yarn (zari, lurex), carbon fibre

Staple and filament

Staple fibresShort fibres measured in centimetres: cotton, wool, flax, and man-made fibre cut to length. They must be twisted together to make a spun yarn.
Filament fibresLong, continuous strands measured in metres or kilometres. Silk is the only natural filament. All man-made fibres are first made as filaments and can be cut into staple.

Activity: how to identify an unknown fibre

In the practical, test the warp and weft separately, because they may be different fibres.

  1. 1
    Look and feel: note lustre, length, crimp and hand. Untwist a yarn: short fibres mean staple; long, smooth strands mean filament.
  2. 2★
    Burning test: hold a few fibres with forceps and bring them slowly to a small flame. Note how they behave near the flame, in it and after removal, the smell and the residue.
    work over a steel tray, away from cloth and the gas stove
  3. 3
    Microscope test: mount a few fibres in a drop of water or glycerine and study the length view; a cross-section needs fibres cut very thin.
  4. 4
    Solubility test: place fibres in a test tube with the reagent and watch whether they dissolve.
    lab only, with gloves and goggles
  5. 5
    Confirm: name the fibre only when two or more tests agree. A blend gives mixed results.

★ one-way, controls the pace

Burning test

FibreNear and in the flameSmellResidue
Cotton, linen, viscose rayon (cellulose)Catch fire quickly, burn with a yellow flame and keep glowing after removal; do not meltBurning paperSoft grey feathery ash (very little from rayon)
Wool and silk (protein)Curl away, burn slowly, sputter, usually go out on their ownBurning hair or feathersBlack, crushable bead
NylonShrinks from the flame, melts and drips, burns slowly, may go outCelery-likeHard grey or tan bead; cannot be crushed
PolyesterShrinks, melts and burns with black, sooty smokeSweetish chemical smellHard black bead; cannot be crushed
AcrylicMelts and burns with sputtering; keeps burningAcrid (sharp, bitter)Hard, irregular black bead
AcetateMelts and burns, drippingVinegarHard black bead

Microscope and solubility tests

FibreUnder the microscope (length view; cross-section)Solubility clue
CottonFlat, twisted ribbon (convolutions); kidney-shaped with a lumenDissolves in 70% sulphuric acid; survives boiling 5% caustic soda
LinenStraight rod with cross-marks (nodes) like bamboo; many-sidedAs cotton
WoolOverlapping scales like roof tiles; round to ovalDissolves in boiling 5% caustic soda and in chlorine bleach; resists dilute acids
SilkSmooth, glass-like rod; triangular with rounded cornersDissolves in boiling 5% caustic soda, in chlorine bleach and in cold concentrated hydrochloric acid
Viscose rayonLengthwise lines (striations); circle with a wavy (serrated) edgeDissolves in 70% sulphuric acid
NylonSmooth rod, often with dark specks of delustrant; round or three-lobedDissolves in 20% hydrochloric acid and in formic acid
PolyesterSmooth rod like nylon; roundResists most reagents; dissolves in hot meta-cresol
AcrylicSmooth or faintly lined; round or dog-bone shapedDissolves in warm dimethylformamide (DMF)
In daily life

Before buying a kitchen apron or hospital uniform, check the fibre on the label or burn one loose thread over a steel plate: cotton turns to ash, but polyester and nylon melt and can stick to skin near a flame.

Exam angle

2 marks: “What is a filament fibre? Give an example.” A long, continuous fibre measured in metres or kilometres. Silk is the only natural filament; nylon and polyester are made as filaments.

5 marks: “Describe the burning test for identifying textile fibres.” Method (forceps, small flame; behaviour near, in and after the flame), then a table for cellulose, protein, nylon and polyester: flame, smell, residue.

10 marks: “Classify textile fibres with suitable examples.” Define fibre; draw the chart (natural: cellulosic, protein, mineral; man-made: regenerated, synthetic, inorganic); two examples per group with Indian ones; staple vs filament.

Remember it

Burning test in three words: cellulose = paper, protein = hair, synthetic = melts to a hard bead.